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1 article(s) from Dorta, Rosa L

Influence of the cis/trans configuration on the supramolecular aggregation of aryltriazoles

Sara Tejera,
Giada Caniglia,
Rosa L. Dorta,
Andrea Favero,
Javier González-Platas and
Jesús T. Vázquez

Beilstein J. Org. Chem. 2019, 15, 2881–2888, doi:10.3762/bjoc.15.282

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Scheme 1: Structures of 4-substituted 1-glucopyranosyltriazoles 1a–g and 2a–g [15].

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Scheme 2: Synthesis of 1,2-cis-/trans-bistriazoles 7a–7g and 8a–8g [15].

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Scheme 3: Compounds 9 (trans) and 10 (cis) [15].

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Scheme 4: Synthesis of (1R,2R)- and (1R,2S)-1,2-bis-(4-(4-bromophenyl)-1H-triazol-1-yl)cyclohexane (12 and 14...

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Figure 1: Tube inversion test: gels formed by compounds 7f, 8f, 10, 12, and 14.

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Figure 2: SEM images of the xerogels of compounds 7f (DMSO, top left), 8f (DMSO/H₂O, 3:1, v/v, top right), 10...

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Figure 3: ORTEP representation of the molecular structure of compound 12 (trans configuration) obtained from ...

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Figure 4: Crystal packing of compound 12 (trans configuration) in DMSO.

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Figure 5: Crystal packing of 10 (cis configuration) in DMSO/H₂O (1:1, v/v). Colored lines: π–π stacking inter...

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Figure 6: CD spectra of compound 10 (cis) in DMSO/H₂O (1:2, v/v) in solution (in black) and as gel (in blue).

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Published 28 Nov 2019

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